What are the most common heat treatment processes for 3D printed metals?

Table of Contents
What Are the Most Common Heat Treatment Processes for 3D Printed Metals?
Overview
1. Stress Relief Annealing
2. Solution Treatment and Aging (STA)
3. Full Annealing
4. Tempering
5. Hot Isostatic Pressing (HIP)
Summary Table of Common Heat Treatments
Recommended Services for Thermal Optimization

What Are the Most Common Heat Treatment Processes for 3D Printed Metals?

Overview

Heat treatment is essential for improving the mechanical properties, microstructure, and dimensional stability of metal parts produced by additive manufacturing processes such as SLM, DMLS, and EBM. These processes often result in residual stresses, anisotropic grain structures, and non-ideal phase distributions. Heat treatment addresses these issues and tailors part performance to application needs.

1. Stress Relief Annealing

This is the most fundamental heat treatment applied to nearly all metal 3D printed parts. It reduces internal residual stress caused by rapid heating and cooling cycles during printing.

  • Ti-6Al-4V: 600–650°C for 2 hours

  • Inconel 718: 870–980°C for 1 hour

  • Tool Steel H13: 600°C for 2–4 hours

Stress relief improves dimensional stability and reduces distortion during post-processing.

2. Solution Treatment and Aging (STA)

STA is essential for precipitation-hardenable alloys to improve strength and fatigue resistance.

  • SUS630/17-4 PH: solution treated at ~1040°C, aged at 482°C (H900 cycle)

  • Inconel 718: solution treated at 980°C, aged at 720°C and 620°C in two steps

  • Tool Steel 1.2709: solution treated at 850°C, aged at 490°C for 6 hours

This process refines microstructure and introduces strengthening precipitates.

3. Full Annealing

Full annealing is used to restore ductility and reduce hardness in work-hardened or stress-prone parts. It promotes equiaxed grain formation and isotropy.

  • SUS316L: 1040–1100°C with controlled cooling

  • Ti-6Al-4V ELI: 700–800°C under vacuum or inert atmosphere

Annealing is particularly useful for improving toughness in medical and pressure-containing parts.

4. Tempering

Tempering follows hardening treatments in tool steels to reduce brittleness and fine-tune hardness levels.

  • Tool Steel D2: tempered at 200–500°C after quenching

  • Tool Steel H13: multiple tempers at 540–620°C for high impact resistance

Tempering adjusts the hardness-to-toughness balance required in tooling and die-casting components.

5. Hot Isostatic Pressing (HIP)

HIP combines high pressure (100–200 MPa) and elevated temperatures to eliminate internal porosity, improve density, and enhance fatigue strength.

  • Ti-6Al-4V: HIP at ~920°C under 100 MPa for 2–4 hours

  • Haynes 230 and Hastelloy X: HIP at 1160°C for turbine applications

HIP is common for critical aerospace and medical parts requiring defect-free internal structures.

Summary Table of Common Heat Treatments

Process

Purpose

Typical Materials

Stress Relief Annealing

Reduce residual stress

Ti-6Al-4V, Inconel 718, H13, 316L

Solution Treatment & Aging

Strengthen via precipitation

17-4 PH, Inconel 718, 1.2709

Full Annealing

Increase ductility, reduce hardness

316L, Ti-6Al-4V ELI

Tempering

Adjust hardness and toughness

Tool Steels (H13, D2, 1.2709)

Hot Isostatic Pressing

Eliminate porosity, improve fatigue

Ti-6Al-4V, Haynes 230, Hastelloy X

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