The timeline for obtaining metallographic analysis results varies significantly, depending on the complexity, and ranges from 3 to 10 business days for most standard analyses. This duration accounts for the meticulous, multi-stage process required to generate reliable microstructural data.
For routine characterization of common materials like Stainless Steel or Aluminum Alloys, the process follows an efficient workflow:
Day 1: Sectioning and Mounting
Precision cutting of the sample using abrasive or diamond saws
Mounting in phenolic or epoxy resin for handling
Required curing time for mounting medium
Day 2: Grinding and Polishing
Progressive abrasive grinding from coarse to fine grits
Diamond suspension polishing to achieve mirror finish
Critical step to remove deformation from sectioning
Day 3: Etching and Microscopy
Chemical etching to reveal microstructure (e.g., Kroll's reagent for Titanium Alloy)
Initial optical microscopy examination
Digital image capture and basic interpretation
Advanced materials and specialized requirements extend the timeline due to additional processing and examination steps:
Materials Requiring Extended Processing:
Superalloy samples (e.g., Inconel 718) often need specialized etchants and examination
Ceramic materials require precise polishing to prevent pull-out
Heat-treated specimens need careful preparation to preserve microstructural features
Advanced Characterization Techniques:
Scanning Electron Microscopy (SEM) adds 1-2 days for high-resolution imaging
Energy Dispersive Spectroscopy (EDS) requires additional 1 day for elemental analysis
Grain size measurement per ASTM E112 adds ½ day for statistical analysis
Image analysis for porosity/phase quantification adds 1 day
Sample Complexity:
Multiple sampling locations from the same component
Large components requiring extensive sectioning
Difficult-to-prepare materials like Copper alloys
Analysis Depth:
Basic qualitative assessment (faster)
Full quantitative analysis with statistical data (slower)
Comparative analysis against multiple standards
Industry-Specific Requirements:
Aerospace and Aviation components often require NADCAP-accredited procedures, adding rigor and time
Medical and Healthcare implant materials necessitate exhaustive documentation
Research and development projects may require iterative examination
Expedited Service (2-3 days): Available for urgent failure analysis or production line decisions, though this may limit analysis scope.
Routine Quality Control (5 days): Standard turnaround for witness coupons from Powder Bed Fusion processes.
Comprehensive Analysis (7-10 days): Full characterization including SEM/EDS, hardness mapping, and quantitative data reporting.
The final report delivery includes:
Digital micrographs with scale markers
Interpretation against relevant ASTM/ISO standards
Comparison to material specifications
Professional conclusions and recommendations
For critical applications in Automotive or Energy and Power sectors, we recommend building additional witness coupons during production to maintain quality control without delaying component delivery.